Preparation and Characterization of Co(II), Ni(II) and Cu(II) New Schiff base complexes derived from acetoacetanilide

  • Muna Abass Hadi, et.al Dep. Of Chemistry, College Of Education for Girls , University of kufa
Keywords: Tridentate, Transition metal complexes ,spectral studies.

Abstract

Solid metal complexes of Co(II), Ni(II),and Cu(II)have been preparation andcharacterization using anew Schiff base (ANPHA) derived from anew azo dye wasβ-[(p-(Nitrophenyl)azo] diketonilideand 4-aminoantipyrine characterized by several techniques, including elemental analysis (C.H.N), molar conductance, magnetic measurements, electronic spectral and IR spectral studies. The data show that these complexes have composition of [ML2] type. Theelectronic spectral, and magnetic susceptibilitydata of the complexes suggest octahedral geometry of all complexes, and the ligand (ANPHA) behaves mono basic tridentate manner, by coordination through the azomethine nitrogen atom and oxygen atoms.

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Published
2017-07-22
How to Cite
et.al, M. A. H. (2017). Preparation and Characterization of Co(II), Ni(II) and Cu(II) New Schiff base complexes derived from acetoacetanilide. Al-Qadisiyah Journal of Pure Science, 19(2), 154-162. Retrieved from https://journalsc.qu.edu.iq/index.php/JOPS/article/view/189
Issue
Vol 19 No 2 (2014)
Section
Articles

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